Fig. 5 X-ray diffractograms of the precipitates formed at 1 M NH4H2PO4, pH 4.0, an Fe/Al molar ratio of 1.2, and different Al concentrations: (a) Fe(II), , (b) Fe(II), , (c) Fe(III), , and (d) Fe(III), . The aging period was 3 wk at 23°C