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Fig. 2. Concentrations of undefined species other than Al13 or Alsym including aggregated or precipitated Al that cannot be detected by NMR (AlNON) (open triangle) and precipitated Al (open circle) as a function of the humic acid carboxyl group versus Al ratios (COOH/Al) after 0.007 and 570 d of aging [10 mmol L–1 hydroxyaluminum (HyA) solution].